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EPA Method 1311, 1312 Semi-Volatiles
Column: DB-5.625, 30m x 0.25mm I.D., 0.50µm Order No.: 122-5632 Carrier: Helium at 35cm/sec Oven: 40°C for 1min, 40-280°C at 12°/min Injector: Splitless, 250°C, 45sec purge activation time, 1µl of 50-100ng/µl standard in methanol Detector B: MSD, 280µC transfer line full scan at m/z 35-400 |
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